LEAD POISONING IN SILVER REFINERS AND ITS PREVENTION

 

 S.K. Tandon, M.  Chatterjee,  A. Bhargava, V. Shukla  and  V. Behari
Industrial Toxicology Research Centre, Lucknow-226001, India

 

ABSTRACT

The refining of silver from old silver ornaments, articles and jeweller’s waste by smelting these with lead scraps for the fabrication of new jewellery is an industry in India. The clinical investigations have shown that 31 out of 50 silver refiners with blood lead, 32.84+1.78 mg/dL (20.3-64.9), decrease in blood d-aminolevulinic acid dehydratase (ALAD) activity and thiamine level and an enhanced urinary ALA were suffering from lead poisoning. Most of these workers have shown anaemia, abdominal colic, blue gum lining and muscular wasting indicative of lead toxicity. Twentyfour workers with high blood lead were equally divided into two groups and given either vitamin B1 (75 mg, once a day) or vitamin C (250 mg, twice a day) for a month. The treatments significantly lowered the blood lead and reduced blood thiamine and copper deficiency. Vitamin C was also effective in reversing the inhibition of blood ALAD activity while the effect of B1 was marginal. The daily intake of these vitamins may prevent the accumulation of lead and reduce its toxic effects in those regularly exposed.

 

INTRODUCTION

Clinical surveys have been conducted to identify cases of occupational lead poisoning among  workers of different lead occupations and population residing in their vicinity. Lead poisoning in adults and children in a family of 18 has been attributed to lead fumes and lead oxide dust emanating during processes of extraction of gold and silver from jeweller’s waste (Joshua et al., 1971). In 8 out of 9 male workers (25-65 yrs) and in 7 workers (25-70 yrs) involved in silver purification by heating impure silver waste and old jewellery together with lead scrapes, with an average blood lead, 120.8 mg/dL (40-210) (Behari et al.,1983) and 113.4 mg/dL (71-208) (Kachru et al., 1989) respectively were found to suffer from lead poisoning. In another survey 23 out of 105 workers (13-60 yrs) engaged in different work`shops of silver industry with blood lead, 60+36 mg/dL were identified on the basis of altered lead sensitive parameters and clinical symptoms  (Flora et al.,1990).

 

METHODOLOGY

A survey was conducted at two different locations of Lucknow city (India) where workers are involved in refining or recovery of silver by smelting old silver ornaments and jeweller’s waste with lead scrapes for the fabrication of new jewellery. In this industry  the workers are exposed to lead and lead oxide vapours in congested workshops without adequate exhaust, ventilation and protective measures. Since most of the workers are unaware of the consequences of lead poisoning, they are at high risk. The blood and urine from 50 workers directly involved in refining silver and soldering of silver jewellery and from 20 workers (control) were collected twice at an interval of one month for determining lead levels and lead sensitive biochemical parameters. They work daily for 8 hrs, six days a week. Blood lead was determined using AAS  (Varian 250 Plus) with graphite atomizer (GTA 97). The levels of zinc, copper, calcium and iron in blood and lead in urine were measured on flame AAS (Parker et al., 1967). The activity of d-aminolevulinic acid dehydratase (ALAD) (Berlin and Schaller, 1974), haemoglobin (Clegg and King, 1942), ascorbic acid (Roe,  1954), thiamine (in terms of pyruvic acid) (Friedmann and Haugen, 1943) in blood and ALA in urine (Davis et al., 1968) were measured. The workers were examined by the physician for clinical symptoms of lead poisoning - abdominal colic, blue gum lining, muscular wasting, tremors  and  through questionaire.

 

RESULTS

The data on hematological investigations and urinalysis of silver refiners and control are summarised in Table 1. Out of 50 silver refiners 31 with high lead, 32.84+1.78 mg/dL have shown an inhibition of blood ALAD activity, a decrease in blood thiamine (indicated by an increase in pyruvic acid) and copper and an enhanced urinary ALA as compared to control, were suspected of lead poisoning. Most of these silver refiners have shown clinical symptoms such as blue gum lining, abdominal colic, anaemia and muscular wasting suggestive of lead poisoning. The remaining 19 silver refiners have also shown significant alterations in lead sensitive parameters and shown separately in Table 1 because of far lower blood lead  (12.66+1.11 mg/dL) and less clinical symptoms. However, they seem to have a risk of developing lead poisoning. The blood zinc and calcium levels in silver refiners and in control were similar and not included in Table 1. The fact that blood levels of thiamine and ascorbic acid decrease in lead intoxication (Bratton et al., 1981, Flora and Tandon, 1995), the administration of these vitamins may reduce their deficiency and prevent lead toxicity. Therefore, 24 out of 31 silver refiners with high blood lead levels who were willing to participate in the treatment programme, were divided equally into two groups. Each worker of first group was given BENALGIS (thiamine propyldisulfide-vitamin B1-Franco-Indian  Remedies  Ltd, Chennai, India)-75 mg, once a day and that of second group VITAMIN C (Wings Pharmaceuticals Pvt. Ltd, New Delhi, India)-250 mg twice a day for one month to investigate their effect on the elevated blood lead and altered lead sensitive parameters. The treatment of workers suspected of lead poisoning with Benalgis reduced blood lead and thiamine and copper deficiencies and further elevated blood iron. The treatment of workers with vitamin C lowered blood lead, reversed the inhibition of blood ALAD activity and reduced thiamine and copper deficiencies. It also elevated blood ascorbic acid and iron levels (Table 2).

 

DISCUSSION

The present findings are consistent with our earlier surveys conducted among silver jewellery workers (Behari et al., 1983, Kachru et al., 1989, Flora et al., 1990) and show that atleast 31 out of 50 workers involved in silver refining were indeed suffering from lead poisoning. The old silver ornaments and jeweller’s waste are smelted with lead scrapes at high temperatures in congested workshops without adequate exhaust system, ventilation and protective measures where workers are exposed to lead fumes and lead oxide dust. Their clothing, hair and food also get contaminated. Besides elevated blood lead, the decreased activity of enzyme blood ALAD and enhanced urinary excretion of its substrate, ALA are the earliest biochemical indicies of lead intoxication (Granick et al., 1972, Sakai et al.,1982  Ong et al.,1990). Apart from these, the silver refiners have shown a definite lowering in blood thiamine and copper and a decreasing trend in blood ascorbic acid as also the early toxic effects of lead affecting the hemopoietic system. There has been a  relationship between these biochemical alterations and clinical symptoms of lead poisoning such as anaemia, abdominal colic, blue gum lining and muscular wasting.

The selected silver refiners with considerably high blood lead levels responded well to one month treatment with  vitamins B1 and C. These vitamins significantly lowered blood lead and reversed lead sensitive hematological alterations. The beneficial effect of thiamine in lead poisoning may be attributed to the formation of their complex(es) followed by excretion. Lead has high affinity for the thiol group (Barton, 1989). Thiamine may undergo conformational transformation in vivo resulting in thiazole open-ring conformation with sulfhydryl (SH) group capable of complexing lead (Olkowski et al., 1991). Ascorbic acid is a lactone containing an enediol group capable of complexing lead to form a poorly ionized but soluble compound. The in vivo ability of ascorbic acid to reduce disulfides to SH containing compounds that are capable of complexing lead and are also required for the stimulation of heme synthetase activity (Kao and Forbes, 1973). The intake of ascorbic acid and zinc in lead exposed workers has been  shown to lower blood lead  and to protect against lead intoxication (Papaioannoa et al., 1978). These vitamins may have bifunctional role, i) to alleviate lead induced vitamin deficiency or disturbance in their metabolism and ii) to act as potential therapeutic complexing agents.

 

CONCLUSION

The occupational lead exposure is preventable if the workers use protective clothing, such as face mask, gloves, respiratory filters and refrain from smoking, eating and drinking in working areas. The workshops should have proper ventilation and efficient exhaust system to reduce the exposure. The daily intake of thiamine and ascorbic acid may prevent accumulation of lead in the body system.

 

REFERENCES

Barton, J.C. (1989) Toxicol. Appl. Pharmacol.  99: 314-322. Behari, J.R., Singh, S. and Tandon, S.K. (1983) Ann. Occup. Hyg. 27:107-109. Berlin, A. and Schaller, K.H.. (1974) Z. Klin. Chem. Klin. Biochem. 12:389-390. Bratton, G.R., Zmudzki, J., Bell, M.C. and Laken, G.W. (1981) Toxicol. Appl. Pharmacol.  59:164-172. Clegg, J.W. and King, E.J. (1942) Brit. Med. J  2:329-333. Davis, J.R., Abrahams, R.H., Fishbein, W.I and  Fabrega,E.A. (1968) Archiv. Environ. Hlth. 17:164-171. Flora, S.J.S., Singh, S. and Tandon, S.K. (1990) J. Environ. Sci. Hlth. A 25: 105-113. Flora, S.J.S. and Tandon S.K. (1995) Tr. Elem. Electro. 12: 131-140. Friedmann, E. and Haugen, E.G. (1943)  J. Biol. Chem. 147: 415-442. Granick, S., Sassa, S. Granick, J.L., Levere,R.D. and Kappas,A.(1972)  Proc.  Nat. Acad. Sci. (USA) 69: 2381-2385. Joshua, G.E., Rathaiken, N. and Benjamin, V. (1971)  Ind. J.  Med. Res. 59: 1496 -1507. Kachru, D.N., Tandon, S.K., Misra, U.K. and Nag, D. (1989)  Ind. J. Med. Sci. 43: 89-91. Kao, R.L.C. and Forbes, R.M. (1973)  Archiv. Environ Hlth.  27: 31-35. Olkowski, A.A., Gooneratne, S.R. and Crestensen, D.A. (1991)  Toxicol. Lett.  59: 153-159. Ong, C.N., Kong, Y.M., Ong, H.Y and Teramoto, K. (1990)  Pharmacol. Toxicol. 66: 23-26. Papaioannoa, R.A., Sohler, R.A. and Pfeiffer, C.C. (1978)  J. Orthonol. Psyt. 7: 1-13. Parker, M.N., Humoller, F.L. and Mahler, D.J. (1967) Clin. Chem. 13: 40-48.Roe, J.H. (1954)  Methods of Biochemical Assays,  ed. Vol. I, pp 115. Interscience Publishers, New York. Sakai, T., Yanagihara, S., Kunugi, Y. and Ushio, K. (1982)  Brit. J. Indus. Med. 39: 382-387.

 


 Table 1. Investigations on lead sensitive biochemical parameters in blood and urine of silver refiners.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

No. of subjects

Age

(year)

                                                   

Haematological investigations

 

 

Urinalysis

 

 

 

Pb

(mg/dL)

Cu

(mg/dL)

 

Fe

(mg/dL)

Hb

(gm/dL)

d-ALAD

(mmole d-ALA/min/L erythrocyte

 

Ascorbic acid

(mg/dL)

Pyruvic acid

(mg/dL)

Pb

(mg/L)

d-ALA

(mg/dL)

Control

20

18-45

9.40±0.92

96.45±9.00

1.86±0.08

12.34±0.42

38.19±1.22

0.46±0.02

0.65±0.02

0.29±0.04

0.15±0.01

 

 

 

(1.9-16.4)

(59.0-225.0)

(1.2-2.5)

(10.0-16.8)

(28.7-50.0)

(0.40-0.58)

(0.52-0.87)

(0.07-0.76)

(0.05-0.21)

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Silver

Refiners

31

18-60

 

32.84±1.78*

(20.3-64.9)

60.39±3.64*

(20.0-122.0)

2.58+0.02*

(1.4-5.4)

11.68±0.31

(8.6-15.4)

 

22.76±1.62*

(10.1-47.1)

0.39±0.03

(0.17-0.66)

0.96±0.04*

(0.53-1.23)

0.37±0.06

(0.08-1.70)

0.32±0.02*

(0.05-0.56)

 

19

16-55

12.66±1.11***

63.50±7.62**

2.36±0.18***

12.54±0.30

22.73±1.75*

0.39±0.03

0.88±0.05*

0.51±0.11

0.21±0.02

 

 

 

(4.9-19.4)

(7.5-155.0)

(1.1-3.4)

(10.1-14.9)

(12.2-42.3)

(0.21-0.75)

(0.63-1.16)

(0.12-1.84)

(0.02-0.35)

 

 

Values represent mean + SE  with range (in parenthesis). The student ‘t’ test was applied  for determining the statistical significance between control and silver refiners, *p<0.001, **p<0.01, ***p<0.05


 

 

 

 

Table 2.  Investigations on the reversal of lead sensitive haematological  and biochemical parameters in silver refiners. 

 

 

Treatment

No. of

Subject

Pb

(mg/dL)

Cu

(mg/dL)

Fe

(mg/dL)

Hb

(gm/dL)

d-ALAD

(mmole

d-ALA/min/L erythrocyte)

Ascorbic acid

(mg/dL)

Pyruvic acid

(mg/dL)

 

 

 

 

 

 

 

 

 

           Pre

Vit.B1

           Post

 

38.50+3.48

61.63+3.82

2.47+0.16

11.98+0.54

 25.53+3.48

0.47+0.05

0.93+0.05

    12

 

 

 

 

 

 

 

 

23.58+2.86**

86.63+6.59**

4.20+0.11*

11.99+0.22

29.29+3.19

0.50+0.04

0.59+0.03*

 

         

 

 

 

 

 

 

 

 

           Pre

Vit.C 

          Post

       

    12         

30.55+1.82

 

49.17+3.61

2.88+0.34

11.53+0.54

21.79+1.54

0.34+0.04

1.02+0.06

    

 

20.21+1.94*

71.93+6.17**

4.18+0.14**

12.20+0.27

28.38+1.47**

0.53+0.03*

0.79+0.04**

 

 

 

 

 

 

 

 

 

 

 

Values represent mean +SE with range (in parenthesis). The student ‘t’ test was applied for determining the statistical significance between pre- and post-treatment of silver refiners, *p<0.001, **p<0.01